C₅₄H₆₉FN₄O₉Si

Base Information

Chemical Name:C₅₄H₆₉FN₄O₉Si
CAS No.:1335557-73-7
Molecular Formula:C₅₄H₆₉FN₄O₉Si
Molecular Weight:965.247
Hs Code.:

C<sub>54</sub>H<sub>69</sub>FN<sub>4</sub>O<sub>9</sub>Si

Synonyms:C₅₄H₆₉FN₄O₉Si

Suppliers and Price of C₅₄H₆₉FN₄O₉Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₆₉FN₄O₉Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₆₉FN₄O₉Si

There total 14 articles about C₅₄H₆₉FN₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1335557-72-6
C₅₃H₆₇FN₄O₉Si

: 1335557-73-7
C₅₄H₆₉FN₄O₉Si

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In water; 1,2-dichloro-ethane; at 20 ℃; for 4.33333h;

Reference yield:

: 394-04-7
5-fluoro-2-methoxybenzoic acid

: 1335557-73-7
C₅₄H₆₉FN₄O₉Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 2 h / -78 - 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

2.2: 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

5.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

6.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

7.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

8.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

8.2: 0.5 h / -78 °C

8.3: -78 - 20 °C

9.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

10.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

11.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 20 °C

12.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil / 5 h / 20 °C

13.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.55 h / -78 °C

13.2: 1 h / -78 - -20 °C

14.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 40 °C / Inert atmosphere

15.1: acetic acid; sodium tris(acetoxy)borohydride / water; 1,2-dichloro-ethane / 4.33 h / 20 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; 1,3-dimethylbarbituric acid; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; water; sec.-butyllithium; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexanes; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;

Reference yield:

: 220901-72-4
3-fluoro-6-methoxy-2-methylbenzoic acid

: 1335557-73-7
C₅₄H₆₉FN₄O₉Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

1.2: 12 h / 25 °C

2.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

3.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

4.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

5.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

7.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

7.2: 0.5 h / -78 °C

7.3: -78 - 20 °C

8.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

9.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

10.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 20 °C

11.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil / 5 h / 20 °C

12.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.55 h / -78 °C

12.2: 1 h / -78 - -20 °C

13.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 40 °C / Inert atmosphere

14.1: acetic acid; sodium tris(acetoxy)borohydride / water; 1,2-dichloro-ethane / 4.33 h / 20 °C

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; 1,3-dimethylbarbituric acid; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; water; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexanes; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;