2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)
CAS No.:76742-38-6
Molecular Formula:C₆₄H₅₃O₁₈P
Molecular Weight:1141.09
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)

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Chemical Property of 2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)

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Technology Process of 2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)

There total 5 articles about 2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₅₂H₄₄O₁₅

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 76742-38-6
2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)

Guidance literature:: In pyridine; chloroform; at 5 ℃;
DOI:10.1016/S0008-6215(00)85906-6

Reference yield:

: 98-88-4
benzoyl chloride

: 76742-38-6
2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) pyridine, room temp., 24 h; 2.) pyridine, chloroform, 0 deg C, then room temp., overnight

2: H₂ / 10percent Pd/C / acetic acid

3: 75 percent / CHCl₃; pyridine / 5 °C

With hydrogen; palladium on activated charcoal; In pyridine; chloroform; acetic acid;
DOI:10.1016/S0008-6215(00)85906-6

Reference yield:

: 76742-36-4
1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol

: 76742-38-6
2,3,4-tri-O-benzoyl-1-O-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-D-ribitol 5-(diphenylphosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) pyridine, room temp., 24 h; 2.) pyridine, chloroform, 0 deg C, then room temp., overnight

2: H₂ / 10percent Pd/C / acetic acid

3: 75 percent / CHCl₃; pyridine / 5 °C

With hydrogen; palladium on activated charcoal; In pyridine; chloroform; acetic acid;
DOI:10.1016/S0008-6215(00)85906-6