4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline

Base Information

Chemical Name:4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline
CAS No.:1584133-21-0
Molecular Formula:C₂₂H₂₉N₃OSi
Molecular Weight:379.577
Hs Code.:

Synonyms:4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline

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Chemical Property of 4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline

Chemical Property:

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Technology Process of 4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline

There total 6 articles about 4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.1%

: 1416374-31-6
4-((tert-butyldimethylsilyl)oxy)benzene-1,2-diamine

: 37904-72-6
2-bromo-1-(4-(dimethylamino)phenyl)ethanone

: 1584133-21-0
4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 4h;

Reference yield:

: 210832-81-8
2,2-dibromo-1-(4-(dimethylamino)phenyl)ethan-1-one

: 1584133-21-0
4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: Diethyl phosphonate; triethylamine / tetrahydrofuran / 0 - 20 °C

2: dimethyl sulfoxide / 4 h / 20 °C

With Diethyl phosphonate; triethylamine; In tetrahydrofuran; dimethyl sulfoxide;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1584133-21-0
4-(6-((tert-butyldimethylsilyl)oxy)quinoxalin-2-yl)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / tetrahydrofuran / 1 h / 20 °C

2: palladium on activated charcoal; hydrogen / methanol; dichloromethane / 7 h / 20 °C

3: dimethyl sulfoxide / 4 h / 20 °C

With 1H-imidazole; palladium on activated charcoal; hydrogen; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide;