N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid

Base Information

Chemical Name:N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid
CAS No.:120229-80-3
Molecular Formula:C₂₃H₃₁NO₃
Molecular Weight:369.504
Hs Code.:

Synonyms:N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid

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Chemical Property of N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid

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Technology Process of N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid

There total 3 articles about N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 120229-67-6
2-(Dimethylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-3-phenylspiro-<4H-chromen-4,1'-cyclopropan>-5-on

: 120262-50-2
5,6,7,8-Tetrahydro-7,7-dimethyl-3-phenylspiro-2,5-dion

: 120229-80-3
N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid

Guidance literature:: With sodium hydrogen sulfate; In dichloromethane; at 50 ℃; for 120h;

Reference yield:

: 110174-72-6
2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate

: 120229-80-3
N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid

Guidance literature:: Multi-step reaction with 2 steps

1: 2) 1,2-diaminoethan / 1) CH₂Cl₂, 4 h, reflux, 2) H₂O

2: 70 percent / 1M aq. NaHSO₄ / CH₂Cl₂ / 120 h / 50 °C

With sodium hydrogen sulfate; ethylenediamine; In dichloromethane;

Reference yield:

: 110174-70-4
5,5-Dimethyl-2-<1-(1-piperidinio)-cyclopropyl>-1-oxo-2-cyclohexen-3-olat

: 120229-80-3
N,N-Diethyl-2-<1-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)cyclopropyl>-2-phenylacetamid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / ethyldiisopropylamine / CH₂Cl₂

2: 2) 1,2-diaminoethan / 1) CH₂Cl₂, 4 h, reflux, 2) H₂O

3: 70 percent / 1M aq. NaHSO₄ / CH₂Cl₂ / 120 h / 50 °C

With sodium hydrogen sulfate; ethylenediamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;