C₄₆H₅₈O₁₁Si

Base Information

Chemical Name:C₄₆H₅₈O₁₁Si
CAS No.:1450741-65-7
Molecular Formula:C₄₆H₅₈O₁₁Si
Molecular Weight:815.045
Hs Code.:

C<sub>46</sub>H<sub>58</sub>O<sub>11</sub>Si

Synonyms:C₄₆H₅₈O₁₁Si

Suppliers and Price of C₄₆H₅₈O₁₁Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₆H₅₈O₁₁Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₆H₅₈O₁₁Si

There total 14 articles about C₄₆H₅₈O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450741-64-6
C₃₇H₅₀O₈Si₂

: 170649-28-2
(3S)-3-<(p-methoxybenzyl)-oxy>-butanal

: 1450741-65-7
C₄₆H₅₈O₁₁Si

Guidance literature:: (3S)-3-<(p-methoxybenzyl)-oxy>-butanal; With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 0.05h; Inert atmosphere; Schlenk technique;

C₃₇H₅₀O₈Si₂; In dichloromethane; at -78 ℃; for 1.5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol402191t

Reference yield:

: 1450741-54-4
3,5-bis((benzyloxy)methoxy)-4-bromobenzaldehyde

: 1450741-65-7
C₄₆H₅₈O₁₁Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 18-crown-6 ether; potassium tert-butylate / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: palladium diacetate; ruphos; potassium carbonate / toluene; water / 1.5 h / 85 °C / Inert atmosphere; Schlenk technique

3.1: tetrahydrofuran; diethyl ether / 0.25 h / -78 - 0 °C / Inert atmosphere; Schlenk technique

4.1: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); potassium osmate; potassium carbonate; methanesulfonamide / water; tert-butyl alcohol / 18 h / 20 °C / Inert atmosphere; Schlenk technique

5.1: iodine; silver trifluoroacetate / chloroform / 1.5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

6.1: N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 24 h / 100 °C / 760.05 Torr / Schlenk technique

7.1: triethylamine; dmap / dichloromethane / 0.25 h / 0 °C / Inert atmosphere; Schlenk technique

8.1: boron trifluoride diethyl etherate / dichloromethane / 0.05 h / -78 °C / Inert atmosphere; Schlenk technique

8.2: 1.5 h / -78 °C / Inert atmosphere; Schlenk technique

With dmap; potassium osmate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; methanesulfonamide; boron trifluoride diethyl etherate; potassium tert-butylate; iodine; palladium diacetate; silver trifluoroacetate; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hexacyanoferrate(III); ruphos; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1.1: |Wittig Olefination / 2.1: |Suzuki Coupling / 4.1: |Sharpless Dihydroxylation / 8.1: |Mukaiyama Aldol Addition / 8.2: |Mukaiyama Aldol Addition;
DOI:10.1021/ol402191t

Reference yield:

: 1450741-62-4
(S)-5,7-bis((benzyloxy)methoxy)-3-((S)-1-hydroxyethyl)-6-((S)-2-methyl-3-oxobutyl)isobenzofuran-1(3H)-one

: 1450741-65-7
C₄₆H₅₈O₁₁Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; dmap / dichloromethane / 0.25 h / 0 °C / Inert atmosphere; Schlenk technique

2.1: boron trifluoride diethyl etherate / dichloromethane / 0.05 h / -78 °C / Inert atmosphere; Schlenk technique

2.2: 1.5 h / -78 °C / Inert atmosphere; Schlenk technique

With dmap; boron trifluoride diethyl etherate; triethylamine; In dichloromethane; 2.1: |Mukaiyama Aldol Addition / 2.2: |Mukaiyama Aldol Addition;
DOI:10.1021/ol402191t