N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide

Base Information

Chemical Name:N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide
CAS No.:143665-49-0
Molecular Formula:C₁₉H₂₂N₂O₅
Molecular Weight:358.394
Hs Code.:

Synonyms:N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide

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Chemical Property of N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide

Chemical Property:

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Technology Process of N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide

There total 4 articles about N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143665-37-6
2-(3-methyl-4-nitrophenyl)acetic acid

: 143665-49-0
N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 3 h / Heating

2: NaHCO₃ / acetone / 6 h / Ambient temperature

With thionyl chloride; sodium hydrogencarbonate; In acetone;
DOI:10.1021/jm00013a017

Reference yield:

: 206874-44-4
2-Diazo-1-(3-methyl-4-nitro-phenyl)-ethanone

: 143665-49-0
N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: Ag₂O, aq. Na₂S₂O₃ / dioxane / 3 h / 75 - 80 °C

2: SOCl₂ / 3 h / Heating

3: NaHCO₃ / acetone / 6 h / Ambient temperature

With thionyl chloride; sodium hydrogencarbonate; sodium thiosulfate; silver(l) oxide; In 1,4-dioxane; acetone;
DOI:10.1021/jm00013a017

Reference yield:

: 35675-46-8
3-methyl-4-nitro-benzoyl chloride

: 143665-49-0
N-(3,4-Dimethoxy-benzyl)-N-methyl-2-(3-methyl-4-nitro-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 3 h / Ambient temperature

2: Ag₂O, aq. Na₂S₂O₃ / dioxane / 3 h / 75 - 80 °C

3: SOCl₂ / 3 h / Heating

4: NaHCO₃ / acetone / 6 h / Ambient temperature

With thionyl chloride; sodium hydrogencarbonate; sodium thiosulfate; silver(l) oxide; In 1,4-dioxane; diethyl ether; acetone;
DOI:10.1021/jm00013a017