(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone

Base Information

Chemical Name:(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone
CAS No.:1330633-73-2
Molecular Formula:C₂₂H₂₇NO₈S
Molecular Weight:465.524
Hs Code.:

Synonyms:(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone

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Chemical Property of (E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone

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Technology Process of (E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone

There total 7 articles about (E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1330634-12-2
(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

: 1330633-73-2
(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone

Guidance literature:: With sodium dithionite; In water; acetone; at 50 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm200570p

Reference yield:

: 22216-44-0
2-(4-methoxy-3-nitrobenzylthio)acetic acid

: 1330633-73-2
(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen peroxide; acetic acid / water / 24 h / 20 °C / Inert atmosphere

2: acetic acid; benzylamine / Inert atmosphere; Reflux

3: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere

With sodium dithionite; dihydrogen peroxide; acetic acid; benzylamine; In water; acetone; 2: Knoevenagel condensation;
DOI:10.1021/jm200570p

Reference yield:

: 592542-51-3
4-methoxy-3-nitrophenylmethanesulfonyl acetic acid

: 1330633-73-2
(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-aminobenzylsulfone

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; benzylamine / Inert atmosphere; Reflux

2: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere

With sodium dithionite; acetic acid; benzylamine; In water; acetone; 1: Knoevenagel condensation;
DOI:10.1021/jm200570p