(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

Base Information

Chemical Name:(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone
CAS No.:1330634-12-2
Molecular Formula:C₂₂H₂₅NO₁₀S
Molecular Weight:495.507
Hs Code.:

Synonyms:(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

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Chemical Property of (E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

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Technology Process of (E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

There total 6 articles about (E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 592542-51-3
4-methoxy-3-nitrophenylmethanesulfonyl acetic acid

: 197304-21-5
4-(4-formyl-3,5-dimethoxyphenoxy)butanoic acid

: 1330634-12-2
(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

Guidance literature:: With acetic acid; benzylamine; Inert atmosphere; Reflux;
DOI:10.1021/jm200570p

Reference yield:

: 22216-44-0
2-(4-methoxy-3-nitrobenzylthio)acetic acid

: 1330634-12-2
(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; acetic acid / water / 24 h / 20 °C / Inert atmosphere

2: acetic acid; benzylamine / Inert atmosphere; Reflux

With dihydrogen peroxide; acetic acid; benzylamine; In water; 2: Knoevenagel condensation;
DOI:10.1021/jm200570p

Reference yield:

: 119-10-8
4-methoxy-3-nitrotoluene

: 1330634-12-2
(E)-2',6'-dimethoxy-4'-phenoxybutanoic acid styryl-4-methoxy-3-nitrobenzylsulfone

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 18 h / Inert atmosphere; Reflux

2: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere

3: dihydrogen peroxide; acetic acid / water / 24 h / 20 °C / Inert atmosphere

4: acetic acid; benzylamine / Inert atmosphere; Reflux

With N-Bromosuccinimide; dihydrogen peroxide; acetic acid; benzylamine; sodium hydroxide; dibenzoyl peroxide; In methanol; tetrachloromethane; water; 4: Knoevenagel condensation;
DOI:10.1021/jm200570p