2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

Base Information

Chemical Name:2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol
CAS No.:116589-04-9
Molecular Formula:C₂₂H₂₅FO₄
Molecular Weight:372.437
Hs Code.:

Synonyms:2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

Suppliers and Price of 2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

There total 10 articles about 2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 3587-60-8
Benzyloxymethyl chloride

: 109034-93-7
3-fluoro-4,6-dimethoxy-1-(methoxymethoxy)-5-methyl-2-(2,4-pentadienyl)benzene

: 116589-04-9
2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

: 2-((Z)-3-Benzyloxymethyl-penta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methyl-phenol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -75 - 0 ℃;

Reference yield:

: 7149-92-0
2,4-dimethoxy-3-methylbenzaldehyde

: 116589-04-9
2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

Guidance literature:: Multi-step reaction with 9 steps

1: 80 percent / Br₂

2: 1.) m-chloroperbenzoic acid, 2.) KOH / 2.) MeOH

3: NaH / dimethylformamide

4: n-BuLi, perchloryl fluoride / diethyl ether

5: HCl / acetone

6: 83 percent / K₂CO₃ / acetone

7: 62 percent / AlCl₃*OEt₂ / CH₂Cl₂ / 1 h / -25 °C

8: NaH

9: 55 percent / n-BuLi / tetrahydrofuran / -75 - 0 °C

With hydrogenchloride; potassium hydroxide; n-butyllithium; perchloryl fluoride; AlCl₃ etherate; bromine; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 5673-07-4
2,6-dimethoxytoluene

: 116589-04-9
2(1-Benzyloxymethylpenta-2,4-dienyl)-3-fluoro-4,6-dimethoxy-5-methylphenol

Guidance literature:: Multi-step reaction with 10 steps

1: 82 percent / TiCl₄

2: 80 percent / Br₂

3: 1.) m-chloroperbenzoic acid, 2.) KOH / 2.) MeOH

4: NaH / dimethylformamide

5: n-BuLi, perchloryl fluoride / diethyl ether

6: HCl / acetone

7: 83 percent / K₂CO₃ / acetone

8: 62 percent / AlCl₃*OEt₂ / CH₂Cl₂ / 1 h / -25 °C

9: NaH

10: 55 percent / n-BuLi / tetrahydrofuran / -75 - 0 °C

With hydrogenchloride; potassium hydroxide; n-butyllithium; perchloryl fluoride; AlCl₃ etherate; bromine; titanium tetrachloride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone;