Technology Process of C34H32F2N4O5
There total 9 articles about C34H32F2N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hypochlorite;
In
dichloromethane; water;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: triethylamine / 1,4-dioxane / 16 h / 80 °C
2.1: trichlorophosphate; N,N-dimethyl-aniline / 36 h / 110 °C / Inert atmosphere
3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3.5 h / 0 - 20 °C
3.2: 16 h / 60 °C
4.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 0.75 h / 20 °C
5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 68 h / 20 °C
6.1: diisobutylaluminium hydride / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
7.1: hydroxylamine hydrochloride; pyridine / 2 h / 20 °C
8.1: sodium hypochlorite / dichloromethane; water / 20 °C
With
pyridine; sodium hypochlorite; lithium hydroxide monohydrate; hydroxylamine hydrochloride; water; diisobutylaluminium hydride; benzotriazol-1-ol; N,N-dimethyl-aniline; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 68 h / 20 °C
2: diisobutylaluminium hydride / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
3: hydroxylamine hydrochloride; pyridine / 2 h / 20 °C
4: sodium hypochlorite / dichloromethane; water / 20 °C
With
pyridine; sodium hypochlorite; hydroxylamine hydrochloride; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water;