N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine

Base Information

Chemical Name:N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine
CAS No.:144155-87-3
Molecular Formula:C₂₅H₂₅ClF₃N₃
Molecular Weight:459.942
Hs Code.:

Synonyms:N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine

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Chemical Property of N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine

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Technology Process of N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine

There total 7 articles about N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.8%

: 144155-69-1
7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone

: 109-55-7
1-amino-3-(dimethylamino)propane

: 144155-87-3
N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Heating;
DOI:10.1021/jm00097a001

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 144155-87-3
N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine

Guidance literature:: Multi-step reaction with 6 steps

1: 32 percent / 50percent aq. NaOH / 72 h / Ambient temperature

2: EtONa / ethanol / 6 h / Heating

3: 2 N NaOH / 2 h / Heating

4: 5 N H₂SO₄ / 4.5 h / Heating

5: 50 percent / piperidine / ethanol / Heating

6: 78.8 percent / p-TsOH*H₂O / toluene / Heating

With piperidine; sodium hydroxide; sulfuric acid; sodium ethanolate; toluene-4-sulfonic acid; In ethanol; toluene;
DOI:10.1021/jm00097a001

Reference yield:

: 20028-53-9
2-amino-5-chlorobenzaldehyde

: 144155-87-3
N'-<7-chloro-1,2,3,4-tetrahydro-3-<4-(trifluoromethyl)phenyl>-1-acridinylidene>-N,N-dimethyl-1,3-propanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / piperidine / ethanol / Heating

2: 78.8 percent / p-TsOH*H₂O / toluene / Heating

With piperidine; toluene-4-sulfonic acid; In ethanol; toluene;
DOI:10.1021/jm00097a001