3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Base Information

Chemical Name:3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide
CAS No.:1311277-69-6
Molecular Formula:C₅₅H₅₇N₅O₁₃
Molecular Weight:996.083
Hs Code.:

3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Synonyms:3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Suppliers and Price of 3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

There total 12 articles about 3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311277-68-5
3,7-anhydro-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-α-D-talo-octonyl chloride

: 101724-61-2
2,4-diamino-6-(benzyloxy)-5-nitrosopyrimidine

: 1311277-69-6
3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at -30 - 25 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.02.102

Reference yield:

: 1311277-67-4
3,7-anhydro-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-α-D-talo-octonic acid

: 1311277-69-6
3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / Inert atmosphere

2: potassium carbonate / tetrahydrofuran / -30 - 25 °C / Inert atmosphere

With oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.02.102

Reference yield:

: 1311277-66-3
2,6-anhydro-1,3,5-tri-O-benzyl-4-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-7,8,9-trideoxy-D-glycero-D-manno-non-8-enitol

: 1311277-69-6
3,7-anhydro-N-(2-amino-6-benzyloxy-5-nitrosopyrimidin-4-yl)-4,6,8-tri-O-benzyl-5-O-(3-O-benzyl-1,2-O-isopropylidene-α-D-ribofuranosuronyl)-2-deoxy-D-glycero-D-talo-octonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 25 °C / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / Inert atmosphere

3: potassium carbonate / tetrahydrofuran / -30 - 25 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.02.102