N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide

Base Information

Chemical Name:N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide
CAS No.:1609657-26-2
Molecular Formula:C₂₇H₃₄N₄O₂
Molecular Weight:446.593
Hs Code.:

Synonyms:N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide

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Chemical Property of N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide

Chemical Property:

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Technology Process of N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide

There total 4 articles about N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18437-58-6
3-methyl-4-pyridinamine

: 1609658-14-1
4-bromo-N-(3-dipropylaminomethyl-4-hydroxybenzyl)benzamide

: 1609657-26-2
N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium tert-butylate; XPhos; In 1,4-dioxane; at 110 ℃; for 18h; Inert atmosphere; Sealed tube;

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 1609657-26-2
N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: HATU; 4-methyl-morpholine / 16 h / 20 °C / Inert atmosphere

2: water; ethanol / 16 h / 100 °C / Inert atmosphere; Sealed tube

3: potassium tert-butylate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; XPhos / 1,4-dioxane / 18 h / 110 °C / Inert atmosphere; Sealed tube

With 4-methyl-morpholine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium tert-butylate; HATU; XPhos; In 1,4-dioxane; ethanol; water;

Reference yield:

: 80311-91-7
N-(4'-bromobenzoyl)-4-hydroxybenzylamine

: 1609657-26-2
N-(3-dipropylaminomethyl-4-hydroxybenzyl)-4-(2-methylpyridin-4-ylamino)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: water; ethanol / 16 h / 100 °C / Inert atmosphere; Sealed tube

2: potassium tert-butylate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; XPhos / 1,4-dioxane / 18 h / 110 °C / Inert atmosphere; Sealed tube

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium tert-butylate; XPhos; In 1,4-dioxane; ethanol; water;