[[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N₂)]₂(μ₂-N₂)]

Base Information

• Chemical Name: [[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N₂)]₂(μ₂-N₂)]
• CAS No.: 1214786-98-7
• Molecular Formula: C₅₀H₅₄Fe₂N₁₂
• Molecular Weight: 934.753

Synonyms:[[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N₂)]₂(μ₂-N₂)]

Chemical Property of [[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N₂)]₂(μ₂-N₂)]

Chemical Property:

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Technology Process of [[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N₂)]₂(μ₂-N₂)]

There total 3 articles about [[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N₂)]₂(μ₂-N₂)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-Diacetylpyridine (1129-30-2) → [[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N2)]2(μ2-N2)] (1214786-98-7)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol / Reflux

2: tetrahydrofuran

3: naphthalene; sodium / tetrahydrofuran / 2 h / Inert atmosphere

With naphthalene; sodium; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;

Reference yield:

diethyl-2,6-pyridinedicarbonyl ester (15658-60-3) → [[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N2)]2(μ2-N2)] (1214786-98-7)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium ethanolate / ethyl acetate / 20 h / Reflux

1.2: 20 h / 0 °C / Reflux

2.1: toluene-4-sulfonic acid / methanol / Reflux

3.1: tetrahydrofuran

4.1: naphthalene; sodium / tetrahydrofuran / 2 h / Inert atmosphere

With naphthalene; sodium ethanolate; sodium; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethyl acetate;

Reference yield:

2,6-bis(1-(2,6-dimethylphenylimino)ethyl)pyridine (204203-16-7) → [[(1,1'-(pyridine-2,6-diyl)bis(N-(2,6-dimethylphenyl)ethan-1-imine))Fe(N2)]2(μ2-N2)] (1214786-98-7)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: naphthalene; sodium / tetrahydrofuran / 2 h / Inert atmosphere

With naphthalene; sodium; In tetrahydrofuran;

upstream raw materials:

2,6-Diacetylpyridine

diethyl-2,6-pyridinedicarbonyl ester

2,6-bis(1-(2,6-dimethylphenylimino)ethyl)pyridine

Downstream raw materials:

[2,6-diacetylpyridinebis(2,6-dimethylphenylimine)]iron(1,1'-divinyltetramethyldisiloxane)

C₃₈H₃₇FeN₃

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