5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide

Base Information

• Chemical Name: 5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide
• CAS No.: 792953-14-1
• Molecular Formula: C₁₀H₉ClN₄O
• Molecular Weight: 236.661
• Mol file: 792953-14-1.mol

Synonyms:5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide

Chemical Property of 5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

5-Amino-1-(2-chlorophenyl)-1H-pyrazole-4-carboxamide 95%+ ^*data from reagent suppliers

Safty Information:

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Technology Process of 5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide

There total 4 articles about 5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5-amino-1-(2-chlorophenyl)-1H-pyrazole-4-carbonitrile (64096-89-5) → 5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide (792953-14-1)

Guidance literature:

With sulfuric acid; at 20 ℃; for 0.5h;

DOI:10.1016/j.bmcl.2012.10.090

Reference yield: 87.0%

α-Cyano-β-dimethylaminoacrylamide (37858-68-7) + (2-chlorophenyl)hydrazine (10449-07-7) → 5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide (792953-14-1)

Guidance literature:

With sodium acetate; In ethanol; for 12h; Reflux;

Reference yield: 79.0%

→ 5-amino-1-(2-chloro-phenyl)-1H-pyrazole-4-carboxylic acid amide (792953-14-1)

Guidance literature:

upstream raw materials:

5-amino-1-(2-chlorophenyl)-1H-pyrazole-4-carbonitrile

α-Cyano-β-dimethylaminoacrylamide

(2-chlorophenyl)hydrazine

Downstream raw materials:

C₁₁H₇ClN₄O

C₁₁H₇ClN₄O₂

C₁₁H₇ClN₄O₂

2-((1-(2-chlorophenyl)-4-hydroxy-1H-pyrazolo[3,4-d]pyrimidin-6-yl)amino)-N-phenylpropanamide

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