4-nitrophenyl 2-nitrophenyl sulfide

Base Information

• Chemical Name: 4-nitrophenyl 2-nitrophenyl sulfide
• CAS No.: 21387-93-9
• Molecular Formula: C₁₂H₈N₂O₄S
• Molecular Weight: 276.273
• Mol file: 21387-93-9.mol

Synonyms:4-nitrophenyl 2-nitrophenyl sulfide

Chemical Property of 4-nitrophenyl 2-nitrophenyl sulfide

Chemical Property:

Purity/Quality:

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• Hazard Codes: 

MSDS Files:

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Technology Process of 4-nitrophenyl 2-nitrophenyl sulfide

There total 10 articles about 4-nitrophenyl 2-nitrophenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

o-nitrothiophenol (4875-10-9) + 4-chlorobenzonitrile (100-00-5) → bis-(2-nitro-phenyl)-sulfide (22100-66-9) + 4-nitrophenyl 2-nitrophenyl sulfide (21387-93-9)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; stirred 5 h, left overnight;

Reference yield: 78.0%

para-nitrobenzenethiol (1849-36-1) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → 4-nitrophenyl 2-nitrophenyl sulfide (21387-93-9)

Guidance literature:

With potassium fluoride impregnated on clinoptilolite; air; In dimethyl sulfoxide; at 110 - 115 ℃; for 10h;

DOI:10.2174/1386207311316050002

Reference yield: 70.0%

2-nitrophenyl phenyl sulfide (4171-83-9) → 1-nitro-2-(phenylsulfinyl)benzene (18739-95-2) + 4-nitrophenyl 2-nitrophenyl sulfide (21387-93-9)

Guidance literature:

With Nitrogen dioxide; In dichloromethane; at -10 ℃; for 2h;

DOI:10.1055/s-2002-31950

upstream raw materials:

1,2-Dinitrobenzene

sodium 4-nitrobenzenethiolate

o-nitrothiophenol

4-chlorobenzonitrile

Downstream raw materials:

2,4'-Dinitrodiphenylsulfoxid

4'-Nitrophenyl-2-nitrosophenylsulfon