diethyl 4-oxo-1-phenylbutylphosphonate

Base Information

Chemical Name:diethyl 4-oxo-1-phenylbutylphosphonate
CAS No.:1155705-57-9
Molecular Formula:C₁₄H₂₁O₄P
Molecular Weight:284.292
Hs Code.:

Synonyms:diethyl 4-oxo-1-phenylbutylphosphonate

Suppliers and Price of diethyl 4-oxo-1-phenylbutylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diethyl 4-oxo-1-phenylbutylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diethyl 4-oxo-1-phenylbutylphosphonate

There total 3 articles about diethyl 4-oxo-1-phenylbutylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1258145-84-4
C₁₆H₂₅O₅P

: 1155705-57-9
diethyl 4-oxo-1-phenylbutylphosphonate

Guidance literature:: With hydrogenchloride; water; In acetone; at 50 ℃; for 3h;
DOI:10.1002/cmdc.201000276

Reference yield: 54.0%

: 201230-82-2
carbon monoxide

: 3095-10-1
diethyl (1-phenylpropa-1,2-dienyl)phosphonate

: 1155705-57-9
diethyl 4-oxo-1-phenylbutylphosphonate

Guidance literature:: With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen; triphenylphosphine; In toluene; at 100 ℃; for 24h; under 36003.6 Torr; Autoclave;
DOI:10.1002/adsc.200800087

Reference yield:

: 1080-32-6
O,O-diethyl benzylphosphonate

: 1155705-57-9
diethyl 4-oxo-1-phenylbutylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; toluene / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / water; acetone / 3 h / 50 °C

With hydrogenchloride; n-butyllithium; In hexane; water; acetone; toluene;
DOI:10.1021/jm200694q