Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

Base Information

Chemical Name:Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside
CAS No.:124710-43-6
Molecular Formula:C₁₉H₂₄Cl₃NO₇
Molecular Weight:484.761
Hs Code.:

Synonyms:Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

Suppliers and Price of Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

There total 1 articles about Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 124710-43-6
Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; water; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(91)80013-D

Reference yield: 97.0%

: 66880-77-1
2-tetradecylhexadecanoic acid

: 124710-43-6
Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

: 124727-98-6
Benzyl 2-deoxy-4,6-O-isopropylidene-3-O-(2-tetradecylhexadecanoyl)-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,2-dichloro-ethane; Ambient temperature;
DOI:10.1016/0008-6215(91)80013-D

Reference yield:

: 124710-43-6
Benzyl 2-deoxy-4,6-O-isopropylidene-2-(2,2,2-trichloroethoxycarbonyl)amino-β-D-glucopyranoside

: 2-Deoxy-4-O-(diphenoxyphosphinyl)-2-dodecanamido-3-O-(2-tetradecylhexadecanoyl)-D-glucopyranose

Guidance literature:: Multi-step reaction with 7 steps

1: 97 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, 4-dimethylaminopyridine / 1,2-dichloro-ethane / Ambient temperature

2: 3.5 g / 80percent aq. acetic acid / 3 h / 50 °C

3: 52 percent / 1,1,3,3-tetramethylurea / CH₂Cl₂ / Ambient temperature

4: 4-dimethylaminopyridine, pyridine / CH₂Cl₂ / Ambient temperature

5: 1.8 g / zinc dust, acetic acid / 3 h / 60 °C

6: 85 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

7: 60 percent / H₂ / 10percent Pd/C / ethanol / Ambient temperature

With pyridine; dmap; hydrogen; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetramethylurea; zinc; palladium on activated charcoal; In ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/0008-6215(91)80013-D