Technology Process of C25H23N3O4
There total 7 articles about C25H23N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H27N3O4;
With
lithium hydroxide monohydrate;
In
tetrahydrofuran; water;
at 20 ℃;
With
hydrogenchloride;
In
tetrahydrofuran; water;
pH=4.0;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; sodium hypophosphite; pyridine / water
2.1: potassium carbonate / methanol
3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 20 °C
4.2: pH 4.0
With
pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hypophosphite; lithium hydroxide monohydrate; potassium carbonate; acetic acid; triethylamine;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 1 h / 110 °C / Inert atmosphere
2.1: sodium nitrite; toluene-4-sulfonic acid; potassium iodide / water; acetonitrile / 3 h / 10 - 20 °C
3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 20 °C
4.2: pH 4.0
With
bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; lithium hydroxide monohydrate; sodium carbonate; toluene-4-sulfonic acid; triethylamine; potassium iodide; sodium nitrite;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; acetonitrile;
1.1: |Suzuki Coupling;