N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol

Base Information

• Chemical Name: N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol
• CAS No.: 77100-96-0
• Molecular Formula: C₂₀H₂₄N₂O₆
• Molecular Weight: 388.42

Synonyms:N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol

Chemical Property of N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol

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Technology Process of N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol

There total 1 articles about N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4'-nitrobenzo-15-crown-5 (60835-69-0) → N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol (77100-96-0)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / dimethylformamide / Ambient temperature

2: 1.) 7.5M HCl, NaNO₂ / 1.) H₂O, 0 deg C

With hydrogenchloride; hydrogen; sodium nitrite; palladium on activated charcoal; In N,N-dimethyl-formamide;

DOI:10.3987/COM-97-S(N)87

Reference yield: 68.0%

N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol (77100-96-0) + Toluene-4-sulfonic acid 2-[2-(2-dodecyloxy-ethoxy)-ethoxy]-ethyl ester (26323-72-8) → (4-{2-[2-(2-Dodecyloxy-ethoxy)-ethoxy]-ethoxy}-phenyl)-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-yl)-diazene

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 80 ℃; for 6h;

DOI:10.3987/COM-97-S(N)87

Reference yield: 51.5%

N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenol (77100-96-0) + ethylene dibromide (106-93-4) → N-(2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)azo-4-phenylbromoethylether

Guidance literature:

With potassium carbonate; for 9h; Reflux;

DOI:10.1039/c4cc04227a

upstream raw materials:

4'-nitrobenzo-15-crown-5

Downstream raw materials:

4-((4-(carboxymethoxy)phenyl)azo)benzo-15-crown-5

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