(2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt

Base Information

Chemical Name:(2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt
CAS No.:108868-91-3
Molecular Formula:C₂H₄O₂*C₁₅H₃₀N₂O₃
Molecular Weight:346.467
Hs Code.:

Synonyms:(2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt

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Chemical Property of (2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt

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Technology Process of (2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt

There total 2 articles about (2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 64-19-7,77671-22-8
acetic acid

: 108868-89-9
(2S,3S)-1-azido-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane

: 108868-91-3
(2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt

Guidance literature:: With hydrogen; palladium on activated charcoal; for 9h;
DOI:10.1021/jm00390a018

Reference yield:

: 107202-61-9
(2R,3S)-3-(t-butoxycarbonylamino)-4-cyclohexyl-1,2-epoxybutane

: 108868-91-3
(2S,3S)-1-amino-2-hydroxy-3-<(tert-butyloxycarbonyl)amino>-4-cyclohexylbutane acetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / sodium azide, ammonium chloride / methanol / 16 h / Heating

2: 87 percent / H₂ / 10percent Pd/C / 9 h

With sodium azide; ammonium chloride; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00390a018