allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane

Base Information

• Chemical Name: allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane
• CAS No.: 474832-62-7
• Molecular Formula: C₁₄H₂₄O₃Si
• Molecular Weight: 268.428
• Mol file: 474832-62-7.mol

Synonyms:allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane

Chemical Property of allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane

There total 1 articles about allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

allyl alcohol (107-18-6) + [(2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)dimethylsilyl]diethylamine (474832-61-6) → allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane (474832-62-7)

Guidance literature:

With methyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃;

DOI:10.1039/b204879e

Reference yield:

allyloxy-(2,6-dimethoxy-1-methyl-cyclohexa-2,5-dienyl)-dimethyl-silane (474832-62-7) → 3-(dimethylphenylsilyl)-1-propanol (68469-62-5)

Guidance literature:

Multi-step reaction with 2 steps

1: di-tert-butyl hyponitrite / hexane / 80 - 85 °C

2: hexane / 25 °C

With trans-di-O-tert-butyl hyponitrite; In hexane;

DOI:10.1039/b204879e

upstream raw materials:

allyl alcohol

[(2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)dimethylsilyl]diethylamine

Downstream raw materials:

3-(dimethylphenylsilyl)-1-propanol