(R)-2-cyclohexyl-4-ethyl-2-thiazoline

Base Information

Chemical Name:(R)-2-cyclohexyl-4-ethyl-2-thiazoline
CAS No.:420134-19-6
Molecular Formula:C₁₁H₁₉NS
Molecular Weight:197.345
Hs Code.:

Synonyms:(R)-2-cyclohexyl-4-ethyl-2-thiazoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-cyclohexyl-4-ethyl-2-thiazoline

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Technology Process of (R)-2-cyclohexyl-4-ethyl-2-thiazoline

There total 2 articles about (R)-2-cyclohexyl-4-ethyl-2-thiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 420133-81-9
(R)-N-[1-(hydroxymethyl)propyl]cyclohexanethiocarboxamide

: 420134-19-6
(R)-2-cyclohexyl-4-ethyl-2-thiazoline

Guidance literature:: With methanesulfonyl chloride; triethylamine; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1016/S0957-4166(01)00481-5

Reference yield:

: 5874-05-5
methyl cyclohexanecarbodithionate

: 420134-19-6
(R)-2-cyclohexyl-4-ethyl-2-thiazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / 48 h / 20 °C

2: 98 percent / mesylchloride; Et₃N / tetrahydrofuran / 0.17 h / 20 °C

With methanesulfonyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0957-4166(01)00481-5

Reference yield: 82.0%

: 75-15-0,12122-00-8
carbon disulfide

: 420134-19-6
(R)-2-cyclohexyl-4-ethyl-2-thiazoline

: 74-88-4
methyl iodide

: 420133-88-6
(R)-methyl-1-(4-ethyl-4,5-dihydro-2-thiazolyl)cyclohexanedithiocarboxylate

Guidance literature:: (R)-2-cyclohexyl-4-ethyl-2-thiazoline; With tert.-butyl lithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 3h;

carbon disulfide; In tetrahydrofuran; at -40 ℃; for 2h;

methyl iodide; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0957-4166(01)00481-5