nonacosa-O-methylagrimoniin

Base Information

• Chemical Name: nonacosa-O-methylagrimoniin
• CAS No.: 82203-02-9
• Molecular Formula: C₁₁₁H₁₁₂O₅₂
• Molecular Weight: 2278.08
• Mol file: 82203-02-9.mol

Synonyms:nonacosa-O-methylagrimoniin

Chemical Property of nonacosa-O-methylagrimoniin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of nonacosa-O-methylagrimoniin

There total 1 articles about nonacosa-O-methylagrimoniin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

agrimoniin (82203-01-8) + dimethyl sulfate (77-78-1) → β-anomer of trideca-O-methylpedunculagin (7045-43-4,79814-67-8,79814-68-9) + α-anomer of trideca-O-methylpedunculagin (7045-43-4,79814-67-8,79814-68-9) + C65H66O31 + nonacosa-O-methylagrimoniin (82203-02-9)

Guidance literature:

With potassium carbonate; In acetone; Further byproducts given; 1.) r.t., 13 h; 2.) reflux, 28 h;

DOI:10.1248/cpb.32.2165

Reference yield:

methanol (67-56-1) + nonacosa-O-methylagrimoniin (82203-02-9) → alpha-D-glucopyranose (492-62-6) + dimethyl penta-O-methyl-m-dehydrodigallate (82220-66-4) + dimethyl (S)-4,4',5,5',6,6'-hexamethoxydiphenoate (4891-62-7,65995-60-0,71307-89-6)

Guidance literature:

DOI:10.1039/c39820000163

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + nonacosa-O-methylagrimoniin (82203-02-9) → 4,5,6,4',5',6'-Hexamethoxy-biphenyl-2,2'-dicarboxylic acid dimethyl ester (4891-62-7,65995-60-0,71307-89-6) + dimethyl penta-O-methyl-m-dehydrodigallate (82220-66-4)

Guidance literature:

With sodium methylate; Yield given. Multistep reaction. Yields of byproduct given; 1.) MeOH, r.t., 12 h;

DOI:10.1248/cpb.32.2165

upstream raw materials:

agrimoniin

dimethyl sulfate

Downstream raw materials:

4,5,6,4',5',6'-Hexamethoxy-biphenyl-2,2'-dicarboxylic acid dimethyl ester

dimethyl penta-O-methyl-m-dehydrodigallate

alpha-D-glucopyranose

dimethyl (S)-4,4',5,5',6,6'-hexamethoxydiphenoate