Technology Process of 3-acetyloxy-2-(2-butenyl)-5-methoxybenzonitrile
There total 7 articles about 3-acetyloxy-2-(2-butenyl)-5-methoxybenzonitrile which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; p-toluenesulfonyl chloride;
at 95 - 100 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 88 percent / H2SO4
2: K2CO3, NaI / various solvent(s) / Heating
3: 2.) 20percent NaOH / 1.) PhNMe2, reflux, 8 h, 2.) overnight
4: 75 percent / pyridine / 24 h / Ambient temperature
5: SOCl2 / diethyl ether / 5 h / Heating
6: NH3 / diethyl ether / 1 h / Ambient temperature
7: 77 percent / p-TsCl, pyridine / 4 h / 95 - 100 °C
With
pyridine; sodium hydroxide; thionyl chloride; sulfuric acid; ammonia; potassium carbonate; p-toluenesulfonyl chloride; sodium iodide;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: K2CO3, NaI / various solvent(s) / Heating
2: 2.) 20percent NaOH / 1.) PhNMe2, reflux, 8 h, 2.) overnight
3: 75 percent / pyridine / 24 h / Ambient temperature
4: SOCl2 / diethyl ether / 5 h / Heating
5: NH3 / diethyl ether / 1 h / Ambient temperature
6: 77 percent / p-TsCl, pyridine / 4 h / 95 - 100 °C
With
pyridine; sodium hydroxide; thionyl chloride; ammonia; potassium carbonate; p-toluenesulfonyl chloride; sodium iodide;
In
diethyl ether;
