2,4,6-Trimethylphenylpropiolaldehyd

Base Information

Chemical Name:2,4,6-Trimethylphenylpropiolaldehyd
CAS No.:73057-38-2
Molecular Formula:C₁₂H₁₂O
Molecular Weight:172.227
Hs Code.:

Synonyms:2,4,6-Trimethylphenylpropiolaldehyd

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Chemical Property of 2,4,6-Trimethylphenylpropiolaldehyd

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Technology Process of 2,4,6-Trimethylphenylpropiolaldehyd

There total 1 articles about 2,4,6-Trimethylphenylpropiolaldehyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73057-39-3
1-(2,4,6-trimethylphenyl)-3,3-diethoxyprop-1-yne

: 73057-38-2
2,4,6-Trimethylphenylpropiolaldehyd

Guidance literature:: (acid hydrolysis);
DOI:10.1016/0040-4020(79)80041-1

Reference yield: 88.0%

: 73057-38-2
2,4,6-Trimethylphenylpropiolaldehyd

: 627-41-8
propargyl alcohol methyl ether

: 1613231-79-0
1-mesityl-6-methoxyhexa-1,4-diyn-3-ol

Guidance literature:: propargyl alcohol methyl ether; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

2,4,6-Trimethylphenylpropiolaldehyd; In tetrahydrofuran; hexane; at -78 - -30 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201310146

Reference yield: 65.0%

: 2009-97-4
ethyl 2-diazo-3-oxobutanoate

: 73057-38-2
2,4,6-Trimethylphenylpropiolaldehyd

: ethyl 2-diazo-5-hydroxy-7-mesityl-3-oxohept-6-ynoate

Guidance literature:: ethyl 2-diazo-3-oxobutanoate; With titanium tetrachloride; triethylamine; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;

2,4,6-Trimethylphenylpropiolaldehyd; In dichloromethane; at -78 ℃; for 8h;
DOI:10.1021/acs.orglett.5b02369