ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate

Base Information

Chemical Name:ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate
CAS No.:112672-52-3
Molecular Formula:C₂₀H₂₂N₄O₄S
Molecular Weight:414.485
Hs Code.:

Synonyms:ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate

There total 9 articles about ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 64-17-5
ethanol

: 53744-76-6
N-phenylthiocarbamoylacetonitrile

: 28663-68-5
ethyl (phenylhydrazono)chloroacetate

: 112672-52-3
ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate

: 5-Cyanomethyl-5-ethoxy-4-phenyl-4,5-dihydro-[1,3,4]thiadiazole-2-carboxylic acid ethyl ester

Guidance literature:: With triethylamine; for 0.25h; Ambient temperature;

Reference yield: 80.0%

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 103-72-0
phenyl isothiocyanate

: 28663-68-5
ethyl (phenylhydrazono)chloroacetate

: 112672-52-3
ethyl 2-[2-aza-1-(ethoxycarbonyl)-2-(phenylamino)vinylthio]-3-aza-3-(phenylamino)prop-2-enoate

: ethyl 2-[5-(ethoxycarbonyl)-3-phenyl(1,3,4-thiadiazolin-2-ylidene)]-3-oxophenylpropanoate

Guidance literature:: ethyl 3-oxo-3-phenylpropionate; phenyl isothiocyanate; With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

ethyl (phenylhydrazono)chloroacetate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1002/hc.10222