(S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate

Base Information

Chemical Name:(S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate
CAS No.:164534-02-5
Molecular Formula:C₂₂H₂₇NO₅
Molecular Weight:385.46
Hs Code.:

Synonyms:(S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate

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Chemical Property of (S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate

Chemical Property:

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Technology Process of (S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate

There total 7 articles about (S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 155499-16-4
2-<3-(allyloxy)phenyl>-1,3-diacetoxypropane

: 164534-02-5
(S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / 1 N aq. NaOH / diisopropyl ether / 24.5 h / porcine pancreatic lipase

2: Huenig's base / CH₂Cl₂ / 26.5 h / Ambient temperature

3: 1 N KOH / methanol / 2 h / 0 °C

4: CrO₃, aq. H₂SO₄ / acetone / 1.5 h / 0 °C

5: aq. NaOH, 1-(3-dimethylaminopropyl)-3-ethyl carbodiimide / tetrahydrofuran / 1.5 h / Ambient temperature

With chromium(VI) oxide; potassium hydroxide; sodium hydroxide; sulfuric acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; di-isopropyl ether; acetone;
DOI:10.1016/0040-4020(96)00804-6

Reference yield:

: 155440-94-1
2-(3-allyloxy)phenyl-1,3-propanediol

: 164534-02-5
(S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / pyridine / 6 h / Ambient temperature

2: 66 percent / 1 N aq. NaOH / diisopropyl ether / 24.5 h / porcine pancreatic lipase

3: Huenig's base / CH₂Cl₂ / 26.5 h / Ambient temperature

4: 1 N KOH / methanol / 2 h / 0 °C

5: CrO₃, aq. H₂SO₄ / acetone / 1.5 h / 0 °C

6: aq. NaOH, 1-(3-dimethylaminopropyl)-3-ethyl carbodiimide / tetrahydrofuran / 1.5 h / Ambient temperature

With pyridine; chromium(VI) oxide; potassium hydroxide; sodium hydroxide; sulfuric acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; di-isopropyl ether; acetone;
DOI:10.1016/0040-4020(96)00804-6

Reference yield:

: 155499-17-5
(S)-3-acetoxy-2-<3-(allyloxy)phenyl>propan-1-ol

: 164534-02-5
(S)-methyl 2-<3-(allyloxy)phenyl>-2-<(benzyloxy)methoxy>-N-methyl-hydroxamate

Guidance literature:: Multi-step reaction with 4 steps

1: Huenig's base / CH₂Cl₂ / 26.5 h / Ambient temperature

2: 1 N KOH / methanol / 2 h / 0 °C

3: CrO₃, aq. H₂SO₄ / acetone / 1.5 h / 0 °C

4: aq. NaOH, 1-(3-dimethylaminopropyl)-3-ethyl carbodiimide / tetrahydrofuran / 1.5 h / Ambient temperature

With chromium(VI) oxide; potassium hydroxide; sodium hydroxide; sulfuric acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1016/0040-4020(96)00804-6