(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

Base Information

Chemical Name:(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one
CAS No.:752225-68-6
Molecular Formula:C₃₁H₄₆O₃S
Molecular Weight:498.77
Hs Code.:

Synonyms:(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

Suppliers and Price of (+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

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Chemical Property of (+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

Chemical Property:

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Technology Process of (+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

There total 1 articles about (+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98540-26-2
1′-(3-methoxyphenyl)-2′-(4′′-methoxyphenyl)ethan-2′-one

: 177583-96-9
1-Bromo-10-(pentylthio)-decane

: 752225-68-6
(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

Guidance literature:: 1′-(3-methoxyphenyl)-2′-(4′′-methoxyphenyl)ethan-2′-one; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

1-Bromo-10-(pentylthio)-decane; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1002/ardp.200400904

Reference yield: 76.0%

: 74-96-4
ethyl bromide

: 752225-68-6
(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

: 752225-74-4
(E/Z)-(+/-)-3-(4-methoxyphenyl)-4-(3-methoxyphenyl)-14-pentylthiotetradec-2-ene

Guidance literature:: ethyl bromide; With iodine; magnesium; In diethyl ether; for 1h; Heating;

(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one; In diethyl ether; for 2h; Heating;
DOI:10.1002/ardp.200400904

Reference yield:

: 752225-68-6
(+/-)-1-(4-methoxyphenyl)-2-(3-methoxyphenyl)-12-pentylthio-dodecan-1-one

: (Z)-3-(4-hydroxyphenyl)-4-(3-hydroxyphenyl)-14-pentylthiotetradec-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg tunings; iodine / diethyl ether / 1 h / Heating

1.2: 76 percent / diethyl ether / 2 h / Heating

2.1: BBr₃ / CH₂Cl₂ / 7 h / -5 - 20 °C

With iodine; boron tribromide; magnesium; In diethyl ether; dichloromethane; 1.1: Grignard reaction;
DOI:10.1002/ardp.200400904