((t)Bu₂PhSiO)3TaH₂

Base Information

Chemical Name:((t)Bu₂PhSiO)3TaH₂
CAS No.:710946-63-7
Molecular Formula:C₄₂H₇₁O₃Si₃Ta
Molecular Weight:889.228
Hs Code.:

((t)Bu<sub>2</sub>PhSiO)3TaH<sub>2</sub>

Synonyms:((t)Bu₂PhSiO)3TaH₂

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Chemical Property of ((t)Bu₂PhSiO)3TaH₂

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Technology Process of ((t)Bu₂PhSiO)3TaH₂

There total 2 articles about ((t)Bu₂PhSiO)3TaH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 710946-62-6
((t)Bu₂PhSiO)3TaCl₂

: 1333-74-0
hydrogen

: 710946-63-7
((t)Bu₂PhSiO)3TaH₂

Guidance literature:: With Na/Hg; In diethyl ether; ((t)Bu2PhSiO)3TaCl2 and Na/Hg in Et2O was stirred under 1 atm H2 for 16 h; solvent was removed in vacuo, residue was suspended in pentane and filtered, solvent was evapd.;
DOI:10.1021/ic035407u

Reference yield:

: 710946-61-5
(t)Bu₂PhSiONa

: 710946-63-7
((t)Bu₂PhSiO)3TaH₂

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: Na/Hg / diethyl ether

With Na/Hg; In diethyl ether; benzene;
DOI:10.1021/ic035407u