7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate

Base Information

• Chemical Name: 7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate
• CAS No.: 941602-60-4
• Molecular Formula: C₃₄H₃₅Cl₃O₁₄
• Molecular Weight: 774.003

Synonyms:7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate

Chemical Property of 7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate

Chemical Property:

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Technology Process of 7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate

There total 1 articles about 7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

14-β-hydroxybaccatin III 1,14-carbonate (318464-43-6) + trifluoroacetyl chloride (76-02-8) → 7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate (941602-60-4)

Guidance literature:

With pyridine; In dichloromethane; at -10 - 0 ℃; for 2.25h;

Reference yield: 92.0%

7-trichloroacetyl-14-hydroxybaccatin III-1,14-carbonate (941602-60-4) + (4S,5R)-N-(tert-butoxycarbonyl)-2-(2,4-dimethoxyphenyl)-4-iso-butyl-5-oxazolidinecarboxylic acid (191276-34-3) → (7-trichloroacetyl)-13-(N-Boc-2-(2,4-dimethoxyphenyl)-4-isobutyl-5-oxazolidinyl)-14-β-hydroxybaccatin-1,14-carbonate (941602-61-5)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 5 ℃; for 3.5h;

upstream raw materials:

14-β-hydroxybaccatin III 1,14-carbonate

trifluoroacetyl chloride

Downstream raw materials:

(7-trichloroacetyl)-13-(N-Boc-2-(2,4-dimethoxyphenyl)-4-isobutyl-5-oxazolidinyl)-14-β-hydroxybaccatin-1,14-carbonate

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