benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside

Base Information

• Chemical Name: benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside
• CAS No.: 59263-37-5
• Molecular Formula: C₅₀H₅₆O₁₁
• Molecular Weight: 832.988

Synonyms:benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside

Chemical Property of benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside

There total 1 articles about benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside (59263-37-5)

Guidance literature:

aus Benzyl-β-D-glucopyranosid 1, Benzylchlorid, KOH;

Reference yield: 95.0%

benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside (59263-37-5) + ethyl iodide (75-03-6) → benzyl 2,6-di-O-benzyl-3-O-ethyl-4-O-(2,6-di-Obenzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.2174/1570178614666170720141917

Reference yield: 90.0%

benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-2,6-di-O-benzyl-β-D-glucopyranoside (59263-37-5) + acetic anhydride (108-24-7) → benzyl 3-O-acetyl-2,6-di-O-benzyl-4-O-(2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside (99388-23-5)

Guidance literature:

With pyridine; dmap; at 20 ℃; for 1h; regioselective reaction;

DOI:10.2174/15701786113109990018

Downstream raw materials:

benzyl 3-O-acetyl-2,6-di-O-benzyl-4-O-(2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

benzyl 2,6-di-O-benzyl-4-O-(2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-3-O-methyl-β-D-glucopyranoside

benzyl 2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl-(1->4)-[2,3,4-tri-O-benzyl-6,7,8,9,10-pentadeoxy-α-L-galacto-decopyranosyl-(1->3)]-2,6-di-O-benzyl-β-D-glucopyranoside

benzyl 2,6-di-O-benzyl-3-O-palmitoyl-4-O-(2,6-di-O-benzyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

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