1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

Base Information

Chemical Name:1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester
CAS No.:205638-45-5
Molecular Formula:C₂₀H₂₃NO₆
Molecular Weight:373.406
Hs Code.:

Synonyms:1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

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Chemical Property of 1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

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Technology Process of 1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

There total 8 articles about 1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 77-78-1
dimethyl sulfate

: 205638-44-4
1-Benzyl-4-hydroxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

: 205638-45-5
1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

Guidance literature:: With potassium carbonate; In acetone; for 2h; Heating;
DOI:10.3987/com-97-7779

Reference yield:

: 99683-30-4
diethyl α-oxoadipate

: 205638-45-5
1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / H₂ / 10percent Pd-C / ethanol / 16 h / 1838.8 Torr

2: 100 percent / diisopropylamine / CHCl₃ / 1.5 h / Heating

3: 95 percent / 60percent NaH / toluene / 0.17 h / Heating

4: 88 percent / MS-5A / tetrahydrofuran / 240 h

5: 77 percent / NaOAc / benzene / 2 h / Heating

6: 81 percent / NaOMe / methanol / 0.67 h / Ambient temperature

7: 80 percent / K₂CO₃ / acetone / 2 h / Heating

With hydrogen; sodium methylate; sodium acetate; sodium hydride; potassium carbonate; diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; chloroform; acetone; toluene; benzene;
DOI:10.3987/com-97-7779

Reference yield:

: 133634-32-9
2-hydroxy-adipic acid diethyl ester

: 205638-45-5
1-Benzyl-4-methoxy-7-methoxymethoxy-2-oxo-2,5,6,7-tetrahydro-1H-[1]pyrindine-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / diisopropylamine / CHCl₃ / 1.5 h / Heating

2: 95 percent / 60percent NaH / toluene / 0.17 h / Heating

3: 88 percent / MS-5A / tetrahydrofuran / 240 h

4: 77 percent / NaOAc / benzene / 2 h / Heating

5: 81 percent / NaOMe / methanol / 0.67 h / Ambient temperature

6: 80 percent / K₂CO₃ / acetone / 2 h / Heating

With sodium methylate; sodium acetate; sodium hydride; potassium carbonate; diisopropylamine; In tetrahydrofuran; methanol; chloroform; acetone; toluene; benzene;
DOI:10.3987/com-97-7779