Technology Process of N-benzyl-N-methyl-1,1-diphenylmethanamine
There total 8 articles about N-benzyl-N-methyl-1,1-diphenylmethanamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
fac-tris(2-phenylpyridinato-N,C2')iridium(III);
In
acetonitrile;
at 20 ℃;
Irradiation;
Inert atmosphere;
DOI:10.1002/ejoc.201901060
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bis(dibenzylideneacetone)-palladium(0); tri-tert-butyl phosphine; caesium carbonate / tetrahydrofuran; toluene / 12 h / 80 - 85 °C
2.1: hydroxylamine hydrochloride; pyridine / methanol / 5 h / Reflux
2.2: 2 h / 0 - 20 °C
3.1: fac-tris(2-phenylpyridinato-N,C2')iridium(III) / acetonitrile / 20 °C / Irradiation; Inert atmosphere
With
pyridine; fac-tris(2-phenylpyridinato-N,C2')iridium(III); tri-tert-butyl phosphine; hydroxylamine hydrochloride; caesium carbonate; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; methanol; toluene; acetonitrile;
DOI:10.1002/ejoc.201901060
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bis(dibenzylideneacetone)-palladium(0); tri-tert-butyl phosphine; caesium carbonate / tetrahydrofuran; toluene / 12 h / 80 - 85 °C
2.1: hydroxylamine hydrochloride; pyridine / methanol / 5 h / Reflux
2.2: 2 h / 0 - 20 °C
3.1: fac-tris(2-phenylpyridinato-N,C2')iridium(III) / acetonitrile / 20 °C / Irradiation; Inert atmosphere
With
pyridine; fac-tris(2-phenylpyridinato-N,C2')iridium(III); tri-tert-butyl phosphine; hydroxylamine hydrochloride; caesium carbonate; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; methanol; toluene; acetonitrile;
DOI:10.1002/ejoc.201901060
