[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate

Base Information

Chemical Name:[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate
CAS No.:1370344-79-8
Molecular Formula:C₅₁H₄₆F₄N₄O₃
Molecular Weight:838.945
Hs Code.:

Synonyms:[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate

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Chemical Property of [5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate

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Technology Process of [5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate

There total 7 articles about [5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₉H₄₄F₄N₄O₂

: 75-36-5
acetyl chloride

: 1370344-79-8
[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 20h;

Reference yield:

: 1370344-76-5
11-(2-ethylhexyl)-8-(2-fluorobenzoyl)-11H-benzo[a]carbazole-5-carbaldehyde

: 1370344-79-8
[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; pyridine / 3 h / 70 °C

2: ammonium acetate; acetic acid / 3 h / 130 °C

3: hydroxylamine hydrochloride; pyridine / 20 h / 120 °C

4: triethylamine / tetrahydrofuran / 20 h / 20 °C

With pyridine; hydroxylamine hydrochloride; ammonium acetate; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran;

Reference yield:

: 1370344-77-6
11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

: 1370344-79-8
[5-(4,5-diphenyl-1H-imidazol-2-yl)-11-(2-ethylhexyl)-11H-benzo[a]carbazol-8-yl]-[2-(2,2,3,3-tetrafluoropropoxy)-phenyl]-methanone oxime O-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate; acetic acid / 3 h / 130 °C

2: hydroxylamine hydrochloride; pyridine / 20 h / 120 °C

3: triethylamine / tetrahydrofuran / 20 h / 20 °C

With pyridine; hydroxylamine hydrochloride; ammonium acetate; acetic acid; triethylamine; In tetrahydrofuran;