11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

Base Information

Chemical Name:11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde
CAS No.:1370344-77-6
Molecular Formula:C₃₅H₃₃F₄NO₃
Molecular Weight:591.646
Hs Code.:

Synonyms:11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

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Chemical Property of 11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

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Technology Process of 11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

There total 5 articles about 11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 76-37-9
2,2,3,3-tetrafluoropropanol

: 1370344-76-5
11-(2-ethylhexyl)-8-(2-fluorobenzoyl)-11H-benzo[a]carbazole-5-carbaldehyde

: 1370344-77-6
11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

Guidance literature:: With pyridine; sodium hydroxide; at 70 ℃; for 3h;

Reference yield:

: 18908-66-2
3-bromomethylheptane

: 1370344-77-6
11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 0 - 20 °C

2.1: trichlorophosphate / 3 h / 0 - 130 °C

3.1: aluminum (III) chloride / dichloromethane / 17 h / 0 - 20 °C

4.1: sodium hydroxide; pyridine / 3 h / 70 °C

With pyridine; aluminum (III) chloride; sodium hydride; sodium hydroxide; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 239-01-0
11H-benzo[a]carbazole

: 1370344-77-6
11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 0 - 20 °C

2.1: trichlorophosphate / 3 h / 0 - 130 °C

3.1: aluminum (III) chloride / dichloromethane / 17 h / 0 - 20 °C

4.1: sodium hydroxide; pyridine / 3 h / 70 °C

With pyridine; aluminum (III) chloride; sodium hydride; sodium hydroxide; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;