Technology Process of 11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde
There total 5 articles about 11-(2-Ethylhexyl)-8-[2-(2,2,3,3-tetrafluoropropoxy)-benzoyl]-11H-benzo[a]carbazole-5-carbaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; sodium hydroxide;
at 70 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
1.2: 0 - 20 °C
2.1: trichlorophosphate / 3 h / 0 - 130 °C
3.1: aluminum (III) chloride / dichloromethane / 17 h / 0 - 20 °C
4.1: sodium hydroxide; pyridine / 3 h / 70 °C
With
pyridine; aluminum (III) chloride; sodium hydride; sodium hydroxide; trichlorophosphate;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
1.2: 0 - 20 °C
2.1: trichlorophosphate / 3 h / 0 - 130 °C
3.1: aluminum (III) chloride / dichloromethane / 17 h / 0 - 20 °C
4.1: sodium hydroxide; pyridine / 3 h / 70 °C
With
pyridine; aluminum (III) chloride; sodium hydride; sodium hydroxide; trichlorophosphate;
In
dichloromethane; N,N-dimethyl-formamide;