[(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]

Base Information

Chemical Name:[(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]
CAS No.:1359998-80-3
Molecular Formula:C₃₀H₂₃AuN₃P
Molecular Weight:653.473
Hs Code.:

Synonyms:[(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]

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Chemical Property of [(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]

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Technology Process of [(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]

There total 4 articles about [(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 1137-68-4
2-(2'-pyridyl)benzimidazole

: 1359998-80-3
[(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; for 24h; Darkness;
DOI:10.3390/ph14010010

Reference yield: 64.0%

: 1359998-79-0
[(2-(2-pyridyl)benzimidazole)Au(triphenylphosphine)][PF₆]

: 1359998-80-3
[(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]

Guidance literature:: With KOH; In methanol; addn. of a soln. of KOH in methanol to a soln. of Au complex in methanol, stirring in the dark for 1 h at room temp.; evapn. in vac., addn. of CH2Cl2, filtration through Celite, concn., addn. of Et2O; elem. anal.;
DOI:10.1021/ic202639t

Reference yield:

: 98-98-6
2-Picolinic acid

: 1359998-80-3
[(2-(2-pyridyl)benzimidazolato)Au(triphenylphosphine)]

Guidance literature:: Multi-step reaction with 3 steps

1: polyphosphoric acid / 180 °C

2: dichloromethane

3: potassium hydroxide / methanol

With potassium hydroxide; In methanol; dichloromethane;
DOI:10.1021/ic500022a