ACRYLONITRILE-2-D1

Base Information

• Chemical Name: ACRYLONITRILE-2-D1
• CAS No.: 4635-82-9
• Molecular Formula: C₃H₃N
• Molecular Weight: 54.0556
• Mol file: 4635-82-9.mol

Synonyms:ACRYLONITRILE-2-D;ACRYLONITRILE-2-D1;ACRYLONITRILE-2-D, 98 ATOM % D

Chemical Property of ACRYLONITRILE-2-D1

Chemical Property:

• Melting Point: −83 °C(lit.)
• Refractive Index: n20/D 1.391(lit.)
• Boiling Point: 77 °C(lit.)
• Flash Point: 32 °F
• PSA: 23.79000
• Density: 0.815 g/mL at 25 °C
• LogP: 0.69598
• Storage Temp.: 0-6°C

Purity/Quality:

Acrylonitrile-2-d ≥98 atom % D, ≥99% (CP), contains hydroquinone as stabilizer ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,T,N
• Statements: 45-46-11-23/24/25-36/37-62-51/53-43-41-63
• Safety Statements: 53-16-23-36/37/39-45-61-26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Acrylonitrile-2-d1 (CAS# 4635-82-9) is a useful isotopically labeled research compound.

Technology Process of ACRYLONITRILE-2-D1

There total 3 articles about ACRYLONITRILE-2-D1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

acrylonitrile (107-13-1,25014-41-9) → acrylonitrile-1-d (4635-82-9)

Guidance literature:

With water-d2; triethylamine; at 20 ℃; for 48h;

DOI:10.1002/jlcr.3603

Reference yield:

C9H9(2)H2N2S(1+)*CH3O4S(1-) → acrylonitrile-1-d (4635-82-9) + C6H7(2)HNS(1+)

Guidance literature:

propylamine; In water; at 25 ℃; Rate constant; elimination, other bases;

DOI:10.1021/ja00223a029

Reference yield:

→ acrylonitrile-1-d (4635-82-9)

Guidance literature:

2-Chloracrylnitril, Zn-Cu, D2O;

DOI:10.1021/jo00422a006

upstream raw materials:

acrylonitrile

Refernces

• 1、 Salin, Alexey V.,Musin, Rashid Z.. "Synthesis of 2-d-acrylamide". . p. 595 - 598. Retrieved 2018.