2--1-chlor-2-(diphenylphosphanylmethyl)propan

Base Information

Chemical Name:2--1-chlor-2-(diphenylphosphanylmethyl)propan
CAS No.:175222-32-9
Molecular Formula:C₃₃H₃₇ClP₂
Molecular Weight:531.057
Hs Code.:

2-<Bis(3,5-dimethylphenyl)phosphanylmethyl>-1-chlor-2-(diphenylphosphanylmethyl)propan

Synonyms:2--1-chlor-2-(diphenylphosphanylmethyl)propan

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Chemical Property of 2--1-chlor-2-(diphenylphosphanylmethyl)propan

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Technology Process of 2--1-chlor-2-(diphenylphosphanylmethyl)propan

There total 1 articles about 2--1-chlor-2-(diphenylphosphanylmethyl)propan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71360-06-0
bis(3,5-dimethylphenyl)phosphine

: 175222-31-8
2-(Brommethyl)-2-(chlormethyl)-1-(methylsulfonyloxy)propan

: 829-85-6
diphenylphosphane

: 175222-32-9
2--1-chlor-2-(diphenylphosphanylmethyl)propan

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) hexane, THF, -50 deg C, 4 h, 2) hexane, THF, 0 deg C, 3 h, to r.t., 18 h;
DOI:10.1002/cber.19961290119

Reference yield: 98.0%

: 100-53-8
phenylmethanethiol

: 175222-32-9
2--1-chlor-2-(diphenylphosphanylmethyl)propan

: 175222-34-1
1-(Benzylsulfanyl)-2--2-(diphenylphosphanylmethyl)propan

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 100 ℃;
DOI:10.1002/cber.19961290119

Reference yield:

: 175222-32-9
2--1-chlor-2-(diphenylphosphanylmethyl)propan

: 2-Bis(3,5-dimethylphenylphosphanylmethyl)-2-(diphenylphosphanylmethyl)-1-propanthiol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / KOtBu / dimethylsulfoxide / 100 °C

2: 68 percent / Li, NH₃ / tetrahydrofuran / -50 °C

With potassium tert-butylate; ammonia; lithium; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/cber.19961290119