3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole

Base Information

Chemical Name:3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole
CAS No.:113707-46-3
Molecular Formula:C₃₀H₃₀N₂O₄S
Molecular Weight:514.645
Hs Code.:

Synonyms:3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole

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Chemical Property of 3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole

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Technology Process of 3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole

There total 5 articles about 3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 113707-44-1
3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>indole

: 98-09-9
benzenesulfonyl chloride

: 113707-46-3
3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In benzene; for 14h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81658-6

Reference yield:

: 60553-33-5
4-(2-methyl-1,3-dioxolan-2-yl)pyridine

: 113707-46-3
3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / methanol / 24 h / Heating

2: 67 percent / 1) HCl, 2) sodium borohydride / H₂O; diethyl ether; methanol / 1 h / Ambient temperature

3: 64 percent / CH₂Cl₂; diethyl ether / 4 h / Ambient temperature

4: 91 percent / aqueous 50percent sodium hydroxide, tetrabutylammonium bisulfate / benzene / 14 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; tetra(n-butyl)ammonium hydrogensulfate; In methanol; diethyl ether; dichloromethane; water; benzene;
DOI:10.1016/S0040-4020(01)81658-6

Reference yield:

: 100-44-7
benzyl chloride

: 113707-46-3
3-<1-benzyl-4-<1,1-(ethylenedioxy)ethyl>-1,2,3,6-tetrahydro-2-pyridyl>-1-(phenylsulfonyl)indole

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / methanol / 24 h / Heating

2: 67 percent / 1) HCl, 2) sodium borohydride / H₂O; diethyl ether; methanol / 1 h / Ambient temperature

3: 64 percent / CH₂Cl₂; diethyl ether / 4 h / Ambient temperature

4: 91 percent / aqueous 50percent sodium hydroxide, tetrabutylammonium bisulfate / benzene / 14 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; tetra(n-butyl)ammonium hydrogensulfate; In methanol; diethyl ether; dichloromethane; water; benzene;
DOI:10.1016/S0040-4020(01)81658-6