(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate

Base Information

Chemical Name:(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate
CAS No.:146499-03-8
Molecular Formula:C₂₂H₃₀O₃
Molecular Weight:342.478
Hs Code.:

Synonyms:(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate

Chemical Property:

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Technology Process of (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate

There total 2 articles about (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 146499-02-7
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydro-1-naphthalenol

: 814-68-6,25189-84-8
acryloyl chloride

: 146499-03-8
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate

Guidance literature:: With triethylamine; dmap; In dichloromethane; 1.) 0 deg C, 1 h, 2.) RT, overnight;
DOI:10.1016/S0040-4020(01)80228-3

Reference yield:

: 117835-14-0,214920-46-4,783334-78-1
bicyclo[2.2.1]hept-5-ene-2-carbonyl chloride

: 146499-02-7
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydro-1-naphthalenol

: 146499-03-8
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate

: (1'R,4a'S,8'S,8a'S,2R)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl endo-2-bicyclo<2.2.1>hept-5-ene carboxylate

: (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl exo-2-bicyclo<2.2.1>hept-5-enecarboxylate

: (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl (S)-endo-2-bicyclo<2.2.1>hept-5-enecarboxylate

Guidance literature:: dmap; In dichloromethane; for 48h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0040-4020(01)80228-3

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 146499-03-8
(1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl prop-2-enoate

: (1'R,4a'S,8'S,8a'S,2R)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl endo-2-bicyclo<2.2.1>hept-5-ene carboxylate

: (1'R,4a'S,8'S,8a'S)-8'-(5''-methoxy-2''-methylphenyl)-8'-methyldecahydronaphthalen-1'-yl exo-2-bicyclo<2.2.1>hept-5-enecarboxylate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 0 ℃; Yield given. Yields of byproduct given; 1.) 45 min, 2.) 5 h;
DOI:10.1016/S0040-4020(01)80228-3