3-METHOXY-4-[(4-METHYLBENZYL)OXY]BENZALDEHYDE

Base Information

• Chemical Name: 3-METHOXY-4-[(4-METHYLBENZYL)OXY]BENZALDEHYDE
• CAS No.: 351066-36-9
• Molecular Formula: C₁₆H₁₆O₃
• Molecular Weight: 256.301
• Hs Code.: 2912499000
• Mol file: 351066-36-9.mol

Synonyms:OTAVA-BB BB7018801959;ZERENEX E/4048097;CHEMBRDG-BB 3003565;ASISCHEM R22370;3-METHOXY-4-[(4-METHYLBENZYL)OXY]BENZALDEHYDE

Chemical Property of 3-METHOXY-4-[(4-METHYLBENZYL)OXY]BENZALDEHYDE

Chemical Property:

• Vapor Pressure: 7.72E-07mmHg at 25°C
• Refractive Index: 1.584
• Boiling Point: 407.1°C at 760 mmHg
• Flash Point: 191.7°C
• PSA: 35.53000
• Density: 1.133g/cm³
• LogP: 3.39510

Purity/Quality:

97% ^*data from raw suppliers

3-Methoxy-4-[(4-methylbenzyl)oxy]benzaldehyde ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-METHOXY-4-[(4-METHYLBENZYL)OXY]BENZALDEHYDE

There total 4 articles about 3-METHOXY-4-[(4-METHYLBENZYL)OXY]BENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

vanillin (121-33-5,8014-42-4) + 4-Methylbenzyl bromide (104-81-4) → 4-((4-methylbenzyl)oxy)-3-methoxybenzaldehyde (351066-36-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

DOI:10.1016/j.poly.2016.05.039

Reference yield: 81.0%

4-methylbenzyl iodide (4484-74-6) + vanillin (121-33-5,8014-42-4) → 4-((4-methylbenzyl)oxy)-3-methoxybenzaldehyde (351066-36-9)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.ejmech.2015.08.054

Reference yield: 80.0%

vanillin (121-33-5,8014-42-4) + 4-Methylbenzyl chloride (104-82-5) → 4-((4-methylbenzyl)oxy)-3-methoxybenzaldehyde (351066-36-9)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 ℃; for 3h; Reflux; Inert atmosphere;

DOI:10.1016/j.bmcl.2014.09.015

upstream raw materials:

vanillin

4-Methylbenzyl chloride

4-methylbenzyl iodide

4-Methylbenzyl bromide

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