1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

Base Information

Chemical Name:1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline
CAS No.:77513-48-5
Molecular Formula:C₂₀H₂₀N₂O₇
Molecular Weight:400.388
Hs Code.:

Synonyms:1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

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Chemical Property of 1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

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Technology Process of 1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

There total 6 articles about 1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 16251-41-5
1-(2'-nitro-4',5'-dimethoxybenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

: 77513-48-5
1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

Guidance literature:: With oxygen; rose bengal; In methanol; for 7h; Irradiation;
DOI:10.1021/jo00147a020

Reference yield:

: 2129-52-4
N-(3,4-dimethoxyphenethyl)-2-(4,5-dimethoxy-2-nitrophenyl)-acetamide

: 77513-48-5
1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Langheld ester (PPE) / CHCl₃ / 24 h / Heating

2: 86 percent / O₂, rose bengal / methanol / 7 h / Irradiation

With ethyl metaphosphate; oxygen; rose bengal; In methanol; chloroform;
DOI:10.1021/jo00147a020

Reference yield:

: 73357-18-3
(4,5-dimethoxy-2-nitrophenyl)acetic acid

: 77513-48-5
1-(4',5'-dimethoxy-2'-nitro-α-oxobenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 0.17 h / 5 °C

2: CH₂Cl₂ / 2 h / 5 °C

3: 81 percent / Langheld ester (PPE) / CHCl₃ / 24 h / Heating

4: 86 percent / O₂, rose bengal / methanol / 7 h / Irradiation

With ethyl metaphosphate; oxygen; rose bengal; In methanol; dichloromethane; chloroform;
DOI:10.1021/jo00147a020