1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

Base Information

Chemical Name:1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole
CAS No.:1219688-95-5
Molecular Formula:C₁₆H₁₈F₃N₃O₂S
Molecular Weight:373.399
Hs Code.:

Synonyms:1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

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Chemical Property of 1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

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Technology Process of 1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

There total 1 articles about 1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1085525-54-7
4-[2-(4-(methanesulfonyl)phenyl)-5-(trifluoromethyl)-2H-pyrazol-3-yl]pyridine

: 1219688-95-5
1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; at 25 ℃; for 20h; under 3102.97 Torr; Autoclave;
DOI:10.1016/j.bmcl.2010.01.014

Reference yield: 23.0%

: 1219688-95-5
1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

: 146563-40-8
4-(nitrooxy)butyl bromide

: 1219688-96-6
1-(4-methanesulfonylphenyl)-5-[1-(4-nitrooxybutyl)piperidin-4-yl]-3-trifluoromethyl-1H-pyrazole

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 24h;
DOI:10.1016/j.bmcl.2010.01.014

Reference yield:

: 1219688-95-5
1-(4-methanesulfonylphenyl)-5-(piperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

: 1219688-98-8
1-(4-methanesulfonylphenyl)-5-(1-nitrosopiperidin-4-yl)-3-trifluoromethyl-1H-pyrazole

Guidance literature:: With nitrogen(II) oxide; sodium methylate; In methanol; acetonitrile; at 25 ℃; under 2068.65 Torr;
DOI:10.1016/j.bmcl.2010.01.014