N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine

Base Information

• Chemical Name: N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine
• CAS No.: 909295-44-9
• Molecular Formula: C₂₈H₄₁N₃O₄
• Molecular Weight: 483.651

Synonyms:N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine

Chemical Property of N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine

Chemical Property:

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Technology Process of N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine

There total 1 articles about N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-N-t-butoxycarbonyl-2-phenylmethyl aziridine (627898-88-8) + (S)-2-(t-butoxycarbonylamino)-3-phenylpropylamine (146552-72-9,179051-72-0) → N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine (909295-44-9)

Guidance literature:

In isopropyl alcohol; at 100 ℃; for 18h; Sealed tube;

DOI:10.1016/j.bmcl.2009.07.118

Reference yield: 90.0%

N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine (909295-44-9) + (fluorenylmethoxy)carbonyl chloride (28920-43-6) → N-[(2R)-2-(tert-butoxycarbonylamino)3-phenylpropyl]-N-[(2S)-2-(tert-butoxycarbonylamino)-3-phenylpropyl]-N-[9-fluorenylmethoxycarbonyl]amine (909295-45-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

N-[(S)-2-(t-butoxycarbonylamino)-3-phenylpropyl][(R)-2-(t-butoxycarbonylamino)-3-phenylpropyl]amine (909295-44-9) → (S)-N1-((R)-2-Amino-3-phenyl-propyl)-3-phenyl-propane-1,2-diamine (714909-31-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2009.07.118

upstream raw materials:

(R)-N-t-butoxycarbonyl-2-phenylmethyl aziridine

(S)-2-(t-butoxycarbonylamino)-3-phenylpropylamine

Downstream raw materials:

N-[(2R)-2-(tert-butoxycarbonylamino)3-phenylpropyl]-N-[(2S)-2-(tert-butoxycarbonylamino)-3-phenylpropyl]-N-[9-fluorenylmethoxycarbonyl]amine

(S)-N¹-((R)-2-Amino-3-phenyl-propyl)-3-phenyl-propane-1,2-diamine

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