3'-deoxy-N⁶-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate>

Base Information

• Chemical Name: 3'-deoxy-N⁶-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate>
• CAS No.: 97776-96-0
• Molecular Formula: C₃₃H₃₀Cl₂N₇O₁₂P
• Molecular Weight: 818.521

Synonyms:3'-deoxy-N⁶-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate>

Chemical Property of 3'-deoxy-N⁶-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate>

Chemical Property:

Purity/Quality:

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Technology Process of 3'-deoxy-N⁶-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate>

There total 8 articles about 3'-deoxy-N⁶-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3'-deoxy-5'-O-(monomethoxytrityl)-N6-<2-(p-nitrophenyl)ethoxycarbonyl>adenosine 2'-<2,5-dichlorphenyl 2-(p-nitrophenyl)ethyl phosphate> (97776-93-7) → 3'-deoxy-N6-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate> (97776-96-0)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; for 0.25h; Ambient temperature;

DOI:10.1002/hlca.19870700808

Reference yield:

2,5-dichlorophenyl phosphorodichloridate (53676-18-9) → 3'-deoxy-N6-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate> (97776-96-0)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine / 0.25 h / Ambient temperature

2: pyridine / 1 h / 0 °C

3: 81 percent / pyridine / 16 h / Ambient temperature

4: 92 percent / TsOH (1percent) / methanol; CH₂Cl₂ / 0.25 h / Ambient temperature

With pyridine; toluene-4-sulfonic acid; In pyridine; methanol; dichloromethane;

DOI:10.1002/hlca.19870700808

Reference yield:

cordycepin (73-03-0) → 3'-deoxy-N6-<2-(p-nitrophenyl)ethoxicarbonyl>adenosine 2'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate> (97776-96-0)

Guidance literature:

Multi-step reaction with 6 steps

1: (NH₄)2SO₄ / dioxane / 3 h / Heating

2: 94 percent / CH₂Cl₂ / 18 h / Ambient temperature

3: 90 percent / pyridine / 18 h / Ambient temperature

4: pyridine / 1 h / 0 °C

5: 81 percent / pyridine / 16 h / Ambient temperature

6: 92 percent / TsOH (1percent) / methanol; CH₂Cl₂ / 0.25 h / Ambient temperature

With pyridine; ammonium sulfate; toluene-4-sulfonic acid; In 1,4-dioxane; pyridine; methanol; dichloromethane;

DOI:10.1002/hlca.19870700808

upstream raw materials:

3'-deoxy-5'-O-(monomethoxytrityl)-N⁶-<2-(p-nitrophenyl)ethoxycarbonyl>adenosine 2'-<2,5-dichlorphenyl 2-(p-nitrophenyl)ethyl phosphate>

2,5-dichlorophenyl phosphorodichloridate

cordycepin

3'-deoxy-5'-O-monomethoxytrityl-6-N-[2-(4-nitrophenyl)-ethoxycarbonyl]-adenosine

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