1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine

Base Information

Chemical Name:1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine
CAS No.:220079-44-7
Molecular Formula:C₂₀H₂₅N₃O₅S
Molecular Weight:422.478
Hs Code.:

Synonyms:1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine

Chemical Property:

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Technology Process of 1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine

There total 5 articles about 1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1849-29-2
1,1,1-trideuteromethanol

: 220079-41-4
N'-Ethyl-N-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid benzyl ester

: 220079-44-7
1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1055/s-1998-2217

Reference yield:

: 4083-64-1
Tosyl isocyanate

: 220079-44-7
1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / CH₂Cl₂

2: 79 percent / Ph₃P, DEAD / tetrahydrofuran

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-1998-2217

Reference yield:

: 127799-53-5
1-[(1,1-dimethylethoxy)carbonyl]-2-[(phenylmethoxy)carbonyl]-2-methylhydrazine

: 220079-44-7
1-(benzyloxycarbonyl)-2-ethyl-1-methyl-2-[(trideuteromethyl)tosylcarbamoyl]hydrazine

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / K₂CO₃, Bu₄NHSO₄, NaOH / benzene / 30 h / Ambient temperature

2: TFA / CH₂Cl₂ / 2 h

3: 99 percent / CH₂Cl₂

4: 79 percent / Ph₃P, DEAD / tetrahydrofuran

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1055/s-1998-2217