2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol

Base Information

Chemical Name:2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol
CAS No.:144968-96-7
Molecular Formula:C₁₇H₁₇F₁₃O₂Si
Molecular Weight:528.386
Hs Code.:

Synonyms:2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol

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Chemical Property of 2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol

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Technology Process of 2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol

There total 1 articles about 2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 355-43-1
n-perfluorohexyl iodide

: 75748-09-3
(4-methoxybenzoyl)trimethylsilane

: 144968-96-7
2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol

Guidance literature:: With ethylmagnesium bromide; Yield given. Multistep reaction; 1) Et₂O, -45 deg C, 0.5 h, 2) Et₂O, -45 to -10 deg C, 2 h;
DOI:10.1055/s-1992-26287

Reference yield: 82.0%

: 144968-96-7
2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol

: 95-54-5
1,2-diamino-benzene

: 3-fluoro-4-(4'-methoxyphenyl)-2-(perfluorobutyl)benzo-1,5-diazepine

Guidance literature:: With magnesium sulfate; In diethyl ether; for 24h; Heating;
DOI:10.1002/ejoc.200300671

Reference yield:

: 144968-96-7
2,2,3,3,4,4,5,5,6,6,7,7,7-Tridecafluoro-1-(4-methoxy-phenyl)-1-trimethylsilanyl-heptan-1-ol

: 151961-18-1
(E)-Perfluorohex-1-enyl 4-methoxyphenyl ketone

Guidance literature:: With potassium fluoride; silica gel; Yield given. Multistep reaction; 1.) DMF, r.t., 1 h, 2.) petroleum ether, CH₂Cl₂, 3 h;
DOI:10.1021/jo00076a028