(+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole

Base Information

• Chemical Name: (+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole
• CAS No.: 94820-24-3
• Molecular Formula: C₃₀H₃₉NO₅
• Molecular Weight: 493.643

Synonyms:(+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole

Chemical Property of (+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole

Chemical Property:

Purity/Quality:

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Technology Process of (+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole

There total 10 articles about (+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-(1-n-butyl-2-hydroxy-3-methoxymethyloxybutyl)-4,5-diphenyloxazole (94820-23-2,94902-03-1,94902-04-2,94902-05-3) + isopentanoyl chloride (108-12-3) → (+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole (94820-24-3)

Guidance literature:

With pyridine;

DOI:10.1021/ja00291a059

Reference yield: 26.0%

2-(1-n-butyl-2-hydroxy-3-methoxymethyloxybutyl)-4,5-diphenyloxazole (94820-23-2,94902-03-1,94902-04-2,94902-05-3) + isopentanoyl chloride (108-12-3) → 2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyloxybutyl)-4,5-diphenyloxazole (94820-24-3,94902-06-4,94902-07-5,94902-08-6) + (+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole (94820-24-3)

Guidance literature:

With pyridine; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)88247-8

Reference yield: 26.0%

2-(1-n-butyl-2-hydroxy-3-methoxymethyloxybutyl)-4,5-diphenyloxazole (94820-23-2,94902-03-1,94902-04-2,94902-05-3) + isopentanoyl chloride (108-12-3) → 2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyloxybutyl)-4,5-diphenyloxazole (94820-24-3,94902-06-4,94902-07-5,94902-08-6) + (+)-(1R,2R,3S)-2-(1-n-butyl-2-isobutylcarbonyloxy-3-methoxymethyl-oxybutyl)-4,5-diphenyloxazole (94820-24-3)

Guidance literature:

With pyridine; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)88247-8

upstream raw materials:

2-(1-n-butyl-2-hydroxy-3-methoxymethyloxybutyl)-4,5-diphenyloxazole

isopentanoyl chloride

2-n-pentyl-4,5-diphenyloxazole

2-methyl-4,5-diphenyloxazole

Downstream raw materials:

(+)-(3S,4R,7R,8R,9S)-3-benzyloxycarbonylamino-7-n-butyl-4,9-dimethyl-1,5-dioxa-8-isobutylcarbonyloxycyclononane-2,6-dione

(+)-(1R,2R,3S)-2-(3-(N-benzyloxycarbonyl-L-threonyloxy)-1-n-butyl-2-isobutylcarbonyloxybutyl)-4,5-diphenyloxazole

(2S,3R)-2-Benzyloxycarbonylamino-3-hydroxy-butyric acid (1S,2R,3R)-3-dibenzoylaminocarbonyl-1-methyl-2-(3-methyl-butyryloxy)-heptyl ester

(-)-(1R,2R,3S)-2-(3-(N-benzyloxycarbonyl-O-t-butyldimethylsilyl-L-threonyloxy)-1-n-butyl-2-isobutylcarbonyloxybutyl)-4,5-diphenyloxazole

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