1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside

Base Information

Chemical Name:1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside
CAS No.:140186-55-6
Molecular Formula:C₃₈H₄₆O₁₀
Molecular Weight:662.777
Hs Code.:

Synonyms:1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside

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Chemical Property of 1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside

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Technology Process of 1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside

There total 4 articles about 1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 96689-78-0
2-pyridyl 2,3,5-tri-O-benzyl-1-thio-β-D-ribofuranoside

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 140186-55-6
1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside

Guidance literature:: With methyl iodide; In dichloromethane;
DOI:10.1016/S0040-4020(01)89016-5

Reference yield:

: 676618-04-5
2-(β-D-ribofuranosylmercapto)pyridine

: 140186-55-6
1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaH / various solvent(s)

2: 67 percent / MeI / CH₂Cl₂

With sodium hydride; methyl iodide; In dichloromethane;
DOI:10.1016/S0040-4020(01)89016-5

Reference yield:

: 16205-59-7
2,3,5-tri-O-benzoyl-1-bromo-α-D-erythro-pentofuranose

: 140186-55-6
1,2:5,6-di-O-isopropylidene-3-O-(2,3,5-tri-O-benzyl-α-D-ribofuranosyl)-α-D-glucofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / K₂CO₃ / toluene; acetone

2: NaOMe / methanol

3: 86 percent / NaH / various solvent(s)

4: 67 percent / MeI / CH₂Cl₂

With sodium methylate; sodium hydride; potassium carbonate; methyl iodide; In methanol; dichloromethane; acetone; toluene;
DOI:10.1016/S0040-4020(01)89016-5